Bruker X8 APEX2 diffractometer | 3903 independent reflections |
Radiation source: fine-focus sealed tube | 2967 reflections with I > 2σ(I) |
graphite | Rint = 0.036 |
φ and ω scans | θmax = 27.5°, θmin = 1.6° |
Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −11→11 |
Tmin = 0.428, Tmax = 0.743 | k = −33→33 |
38010 measured reflections | l = −9→10 |