C1—N1 | 1.326 (9) | C16—H16 | 0.9300 |
C1—C2 | 1.393 (10) | C17—C18 | 1.378 (12) |
C1—H1 | 0.9300 | C17—H17 | 0.9300 |
C2—C3 | 1.362 (12) | C18—C19 | 1.389 (9) |
C2—H2 | 0.9300 | C18—H18 | 0.9300 |
C3—C4 | 1.391 (12) | C19—N4 | 1.366 (8) |
C3—H3 | 0.9300 | C19—C20 | 1.493 (9) |
C4—C5 | 1.402 (9) | C20—N5 | 1.288 (9) |
C4—H4 | 0.9300 | C20—C21 | 1.477 (10) |
C5—N1 | 1.346 (8) | C21—H21A | 0.9600 |
C5—C6 | 1.492 (10) | C21—H21B | 0.9600 |
C6—N2 | 1.277 (9) | C21—H21C | 0.9600 |
C6—C7 | 1.501 (9) | C22—O2 | 1.285 (8) |
C7—H7A | 0.9600 | C22—N6 | 1.346 (8) |
C7—H7B | 0.9600 | C22—C23 | 1.476 (9) |
C7—H7C | 0.9600 | C23—C28 | 1.389 (10) |
C8—O1 | 1.262 (8) | C23—C24 | 1.410 (9) |
C8—N3 | 1.321 (8) | C24—C25 | 1.390 (12) |
C8—C9 | 1.508 (9) | C24—H24 | 0.9300 |
C9—C10 | 1.381 (10) | C25—C26 | 1.396 (16) |
C9—C14 | 1.393 (10) | C25—H25 | 0.9300 |
C10—C11 | 1.376 (11) | C26—C27 | 1.355 (13) |
C10—H10 | 0.9300 | C26—H26 | 0.9300 |
C11—C12 | 1.404 (12) | C27—C28 | 1.394 (10) |
C11—H11 | 0.9300 | C27—H27 | 0.9300 |
C12—C13 | 1.358 (11) | C28—H28 | 0.9300 |
C12—H12 | 0.9300 | N1—Ni1 | 2.099 (5) |
C13—C14 | 1.393 (10) | N2—N3 | 1.380 (8) |
C13—H13 | 0.9300 | N2—Ni1 | 1.992 (5) |
C14—H14 | 0.9300 | N4—Ni1 | 2.091 (5) |
C15—N4 | 1.329 (9) | N5—N6 | 1.359 (8) |
C15—C16 | 1.375 (12) | N5—Ni1 | 1.995 (5) |
C15—H15 | 0.9300 | Ni1—O1 | 2.098 (5) |
C16—C17 | 1.376 (12) | Ni1—O2 | 2.098 (5) |
N1—C1—C2 | 123.4 (7) | N5—C20—C19 | 112.9 (6) |
N1—C1—H1 | 118.3 | C21—C20—C19 | 120.7 (6) |
C2—C1—H1 | 118.3 | C20—C21—H21A | 109.5 |
C3—C2—C1 | 117.9 (7) | C20—C21—H21B | 109.5 |
C3—C2—H2 | 121.1 | H21A—C21—H21B | 109.5 |
C1—C2—H2 | 121.1 | C20—C21—H21C | 109.5 |
C2—C3—C4 | 120.1 (6) | H21A—C21—H21C | 109.5 |
C2—C3—H3 | 120.0 | H21B—C21—H21C | 109.5 |
C4—C3—H3 | 120.0 | O2—C22—N6 | 124.7 (6) |
C3—C4—C5 | 118.6 (7) | O2—C22—C23 | 119.3 (5) |
C3—C4—H4 | 120.7 | N6—C22—C23 | 116.0 (5) |
C5—C4—H4 | 120.7 | C28—C23—C24 | 118.7 (7) |
N1—C5—C4 | 121.0 (6) | C28—C23—C22 | 120.6 (6) |
N1—C5—C6 | 115.9 (5) | C24—C23—C22 | 120.6 (6) |
C4—C5—C6 | 123.1 (6) | C25—C24—C23 | 118.8 (9) |
N2—C6—C5 | 112.9 (6) | C25—C24—H24 | 120.6 |
N2—C6—C7 | 123.8 (7) | C23—C24—H24 | 120.6 |
C5—C6—C7 | 123.3 (6) | C24—C25—C26 | 121.8 (8) |
C6—C7—H7A | 109.5 | C24—C25—H25 | 119.1 |
C6—C7—H7B | 109.5 | C26—C25—H25 | 119.1 |
H7A—C7—H7B | 109.5 | C27—C26—C25 | 118.6 (8) |
C6—C7—H7C | 109.5 | C27—C26—H26 | 120.7 |
H7A—C7—H7C | 109.5 | C25—C26—H26 | 120.7 |
H7B—C7—H7C | 109.5 | C26—C27—C28 | 121.3 (9) |
O1—C8—N3 | 127.4 (6) | C26—C27—H27 | 119.3 |
O1—C8—C9 | 117.8 (5) | C28—C27—H27 | 119.3 |
N3—C8—C9 | 114.7 (5) | C23—C28—C27 | 120.7 (7) |
C10—C9—C14 | 118.2 (7) | C23—C28—H28 | 119.7 |
C10—C9—C8 | 122.0 (6) | C27—C28—H28 | 119.7 |
C14—C9—C8 | 119.8 (6) | C1—N1—C5 | 119.0 (6) |
C11—C10—C9 | 121.8 (8) | C1—N1—Ni1 | 128.6 (5) |
C11—C10—H10 | 119.1 | C5—N1—Ni1 | 112.3 (4) |
C9—C10—H10 | 119.1 | C6—N2—N3 | 120.7 (5) |
C10—C11—C12 | 119.5 (7) | C6—N2—Ni1 | 120.3 (5) |
C10—C11—H11 | 120.2 | N3—N2—Ni1 | 118.7 (4) |
C12—C11—H11 | 120.2 | C8—N3—N2 | 107.7 (5) |
C13—C12—C11 | 119.2 (7) | C15—N4—C19 | 118.3 (6) |
C13—C12—H12 | 120.4 | C15—N4—Ni1 | 129.0 (5) |
C11—C12—H12 | 120.4 | C19—N4—Ni1 | 112.5 (4) |
C12—C13—C14 | 121.3 (7) | C20—N5—N6 | 120.9 (5) |
C12—C13—H13 | 119.4 | C20—N5—Ni1 | 119.7 (5) |
C14—C13—H13 | 119.4 | N6—N5—Ni1 | 118.8 (4) |
C13—C14—C9 | 120.1 (7) | C22—N6—N5 | 109.5 (5) |
C13—C14—H14 | 120.0 | N2—Ni1—N5 | 174.5 (2) |
C9—C14—H14 | 120.0 | N2—Ni1—N4 | 105.6 (2) |
N4—C15—C16 | 123.5 (7) | N5—Ni1—N4 | 78.4 (2) |
N4—C15—H15 | 118.3 | N2—Ni1—O1 | 76.29 (19) |
C16—C15—H15 | 118.3 | N5—Ni1—O1 | 99.93 (19) |
C15—C16—C17 | 118.2 (7) | N4—Ni1—O1 | 92.3 (2) |
C15—C16—H16 | 120.9 | N2—Ni1—O2 | 99.56 (19) |
C17—C16—H16 | 120.9 | N5—Ni1—O2 | 76.7 (2) |
C16—C17—C18 | 120.1 (7) | N4—Ni1—O2 | 154.7 (2) |
C16—C17—H17 | 120.0 | O1—Ni1—O2 | 96.6 (2) |
C18—C17—H17 | 120.0 | N2—Ni1—N1 | 78.2 (2) |
C17—C18—C19 | 118.7 (7) | N5—Ni1—N1 | 105.9 (2) |
C17—C18—H18 | 120.6 | N4—Ni1—N1 | 89.5 (2) |
C19—C18—H18 | 120.6 | O1—Ni1—N1 | 153.90 (19) |
N4—C19—C18 | 121.2 (6) | O2—Ni1—N1 | 92.8 (2) |
N4—C19—C20 | 115.2 (5) | C8—O1—Ni1 | 109.5 (4) |
C18—C19—C20 | 123.6 (6) | C22—O2—Ni1 | 110.1 (4) |
N5—C20—C21 | 126.3 (7) | ||
N1—C1—C2—C3 | −0.8 (11) | C18—C19—N4—Ni1 | 176.5 (5) |
C1—C2—C3—C4 | 0.3 (11) | C20—C19—N4—Ni1 | −1.5 (6) |
C2—C3—C4—C5 | 1.2 (11) | C21—C20—N5—N6 | −1.5 (10) |
C3—C4—C5—N1 | −2.3 (10) | C19—C20—N5—N6 | 174.9 (5) |
C3—C4—C5—C6 | 176.2 (6) | C21—C20—N5—Ni1 | 170.3 (6) |
N1—C5—C6—N2 | 5.6 (8) | C19—C20—N5—Ni1 | −13.3 (7) |
C4—C5—C6—N2 | −173.0 (6) | O2—C22—N6—N5 | −1.3 (8) |
N1—C5—C6—C7 | −173.6 (6) | C23—C22—N6—N5 | 177.0 (5) |
C4—C5—C6—C7 | 7.8 (10) | C20—N5—N6—C22 | 175.0 (6) |
O1—C8—C9—C10 | −161.4 (7) | Ni1—N5—N6—C22 | 3.1 (6) |
N3—C8—C9—C10 | 16.3 (10) | C6—N2—Ni1—N4 | 92.0 (5) |
O1—C8—C9—C14 | 16.8 (9) | N3—N2—Ni1—N4 | −94.3 (4) |
N3—C8—C9—C14 | −165.5 (6) | C6—N2—Ni1—O1 | −179.5 (5) |
C14—C9—C10—C11 | −1.0 (13) | N3—N2—Ni1—O1 | −5.7 (4) |
C8—C9—C10—C11 | 177.2 (8) | C6—N2—Ni1—O2 | −85.0 (5) |
C9—C10—C11—C12 | 1.2 (14) | N3—N2—Ni1—O2 | 88.7 (4) |
C10—C11—C12—C13 | −0.5 (13) | C6—N2—Ni1—N1 | 5.9 (5) |
C11—C12—C13—C14 | −0.2 (12) | N3—N2—Ni1—N1 | 179.6 (5) |
C12—C13—C14—C9 | 0.3 (11) | C20—N5—Ni1—N4 | 10.0 (5) |
C10—C9—C14—C13 | 0.3 (10) | N6—N5—Ni1—N4 | −178.1 (4) |
C8—C9—C14—C13 | −178.0 (6) | C20—N5—Ni1—O1 | −80.3 (5) |
N4—C15—C16—C17 | −2.3 (13) | N6—N5—Ni1—O1 | 91.6 (4) |
C15—C16—C17—C18 | 1.7 (13) | C20—N5—Ni1—O2 | −174.8 (5) |
C16—C17—C18—C19 | 0.8 (11) | N6—N5—Ni1—O2 | −2.8 (4) |
C17—C18—C19—N4 | −2.8 (9) | C20—N5—Ni1—N1 | 96.1 (5) |
C17—C18—C19—C20 | 175.0 (6) | N6—N5—Ni1—N1 | −91.9 (4) |
N4—C19—C20—N5 | 9.3 (7) | C15—N4—Ni1—N2 | −14.2 (7) |
C18—C19—C20—N5 | −168.7 (6) | C19—N4—Ni1—N2 | 172.2 (4) |
N4—C19—C20—C21 | −174.1 (6) | C15—N4—Ni1—N5 | 169.7 (7) |
C18—C19—C20—C21 | 8.0 (9) | C19—N4—Ni1—N5 | −3.8 (4) |
O2—C22—C23—C28 | 0.9 (9) | C15—N4—Ni1—O1 | −90.6 (6) |
N6—C22—C23—C28 | −177.6 (6) | C19—N4—Ni1—O1 | 95.8 (4) |
O2—C22—C23—C24 | −176.2 (6) | C15—N4—Ni1—O2 | 158.8 (6) |
N6—C22—C23—C24 | 5.4 (9) | C19—N4—Ni1—O2 | −14.7 (7) |
C28—C23—C24—C25 | −0.6 (11) | C15—N4—Ni1—N1 | 63.3 (6) |
C22—C23—C24—C25 | 176.5 (7) | C19—N4—Ni1—N1 | −110.2 (4) |
C23—C24—C25—C26 | −1.3 (14) | C1—N1—Ni1—N2 | 173.1 (6) |
C24—C25—C26—C27 | 3.2 (16) | C5—N1—Ni1—N2 | −2.1 (4) |
C25—C26—C27—C28 | −3.1 (14) | C1—N1—Ni1—N5 | −10.8 (6) |
C24—C23—C28—C27 | 0.8 (10) | C5—N1—Ni1—N5 | 174.0 (4) |
C22—C23—C28—C27 | −176.3 (6) | C1—N1—Ni1—N4 | 67.0 (6) |
C26—C27—C28—C23 | 1.1 (12) | C5—N1—Ni1—N4 | −108.2 (4) |
C2—C1—N1—C5 | −0.3 (10) | C1—N1—Ni1—O1 | 161.2 (5) |
C2—C1—N1—Ni1 | −175.2 (5) | C5—N1—Ni1—O1 | −14.0 (7) |
C4—C5—N1—C1 | 1.8 (9) | C1—N1—Ni1—O2 | −87.8 (6) |
C6—C5—N1—C1 | −176.8 (6) | C5—N1—Ni1—O2 | 97.0 (4) |
C4—C5—N1—Ni1 | 177.6 (5) | N3—C8—O1—Ni1 | −1.3 (8) |
C6—C5—N1—Ni1 | −1.0 (6) | C9—C8—O1—Ni1 | 176.1 (4) |
C5—C6—N2—N3 | 178.5 (5) | N2—Ni1—O1—C8 | 3.6 (4) |
C7—C6—N2—N3 | −2.3 (10) | N5—Ni1—O1—C8 | −172.2 (4) |
C5—C6—N2—Ni1 | −7.9 (7) | N4—Ni1—O1—C8 | 109.1 (4) |
C7—C6—N2—Ni1 | 171.3 (5) | O2—Ni1—O1—C8 | −94.6 (4) |
O1—C8—N3—N2 | −3.2 (9) | N1—Ni1—O1—C8 | 15.6 (7) |
C9—C8—N3—N2 | 179.4 (5) | N6—C22—O2—Ni1 | −0.9 (7) |
C6—N2—N3—C8 | −179.8 (6) | C23—C22—O2—Ni1 | −179.2 (4) |
Ni1—N2—N3—C8 | 6.5 (7) | N2—Ni1—O2—C22 | −173.9 (4) |
C16—C15—N4—C19 | 0.4 (11) | N5—Ni1—O2—C22 | 1.9 (4) |
C16—C15—N4—Ni1 | −172.8 (6) | N4—Ni1—O2—C22 | 12.9 (7) |
C18—C19—N4—C15 | 2.2 (9) | O1—Ni1—O2—C22 | −96.8 (4) |
C20—C19—N4—C15 | −175.8 (6) | N1—Ni1—O2—C22 | 107.6 (4) |