| Bruker SMART APEXII diffractometer | 3600 independent reflections |
| Radiation source: fine-focus sealed tube | 3352 reflections with I > 2σ |
| graphite | Rint = 0.093 |
| ω scans | θmax = 26.3°, θmin = 2.1° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −12→10 |
| Tmin = 0.751, Tmax = 0.821 | k = −22→24 |
| 5679 measured reflections | l = −15→13 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.