| Bruker SMART APEX diffractometer | 1169 independent reflections |
| Radiation source: fine-focus sealed tube | 1168 reflections with I > 2σ(I) |
| graphite | Rint = 0.030 |
| ω scans | θmax = 70.8°, θmin = 6.1° |
| Absorption correction: multi-scan (SADABS; Bruker, 2003) | h = −6→5 |
| Tmin = 0.707, Tmax = 0.900 | k = −11→11 |
| 7227 measured reflections | l = −13→13 |
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