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. Author manuscript; available in PMC: 2011 Apr 14.
Published in final edited form as: J Am Chem Soc. 2010 Apr 14;132(14):5030–5032. doi: 10.1021/ja101256v

Table 1.

Catalyst optimization

graphic file with name nihms252453t1.jpg
graphic file with name nihms252453t2.jpg

Optimization reactions performed on 0.033 mmol scale.

a)

Yields determined by GC analysis relative to an internal standard.

b)

Enantiomeric excess determined by SFC analysis on commercial chiral columns.