TABLE 1.
Data collection and refinement statistics
Values for the highest resolution shell are shown in parentheses.
| Construct | 2B4dH |
| Crystal space group | P31 |
| Crystal unit cell parameters | |
| a = b | 91.47 Å |
| c | 150.40 Å |
| α = β | 90 |
| γ | 120 |
| Data collection statistics | |
| Beamline | SSRL 7-1 |
| Wavelength | 0.97 Å |
| Resolution range | 150.0 to 1.76 Å |
| Completeness | 97.9% (96.8%) |
| Redundancy | 4.7 (4.5) |
| Rmerge | 6 (34%) |
| I/s | 7.9 (2.2) |
| No. of observations | 643,945 |
| No. of unique reflections | 135,654 |
| Refinement statistics | |
| R-factor | 19.6% |
| R-free | 22.3% |
| r.m.s.d. | |
| Bond lengths | 0.013 Å |
| Bond angles | 1.443° |
| Average B-factor | 26.276 Å2 |
| Ramachandran plot | |
| Preferred | 97.8% |
| Allowed | 100% |