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. Author manuscript; available in PMC: 2011 Sep 24.
Published in final edited form as: J Nat Prod. 2010 Sep 24;73(9):1524–1528. doi: 10.1021/np100351p

Table 1.

13C NMR Spectroscopic Data of Compounds 1-6 (C5D5N)a

C 1 2 3 4 5 6
1 82.3 83.7 83.5 83.7 82.9 83.5
2 37.3 37.4 37.6 37.3 37.3 37.8
3 67.7 68.2 68.0 68.1 68.0 68.2
4 43.6 43.9 44.3 43.9 43.7 43.9
5 162.7 139.6 142.8 139.5 142.6 139.6
6 128.1 125.0 129.0 124.9 128.5 124.8
7 202.0 32.2 65.0 32.1 64.6 32.1
8 42.0 33.2 42.8 33.1 42.2 33.2
9 50.1 50.4 50.8 50.2 50.4 50.4
10 43.6 43.1 44.1 43.0 43.7 43.0
11 23.8 24.0 24.2 24.0 23.5 24.0
12 40.0 40.2 40.2 40.1 40.1 40.5
13 40.8 40.2 40.4 40.0 40.1 40.3
14 49.0 56.7 39.2 56.6 40.0 56.9
15 34.4 32.5 32.8 32.4 32.4 32.5
16 81.6 81.5 82.2 81.9 81.5 81.3
17 62.0 62.9 63.4 62.4 63.0 62.9
18 16.8 16.9 17.0 16.6 16.4 16.8
19 13.3 15.1 15.4 15.0 14.9 15.1
20 42.6 42.0 42.4 42.1 42.2 42.6
21 15.0 14.9 14.4 14.9 15.0 14.9
22 109.7 109.5 109.8 111.8 109.8 109.8
23 26.5 33.4 33.7 43.6 26.5 26.5
24 26.3 29.0 29.4 67.3 26.3 26.3
25 27.7 144.7 145.0 149.4 27.6 27.7
26 65.2 65.2 65.3 64.6 65.7 65.2
27 16.5 108.7 108.9 106.5 16.7 16.4
Ara-1′ 101.8 100.3 100.3 100.3 102.3 102.3
 2′ 76.0 75.9 76.3 76.2 72.9 71.7
 3′ 75.2 75.2 75.5 75.2 74.0 84.0
 4′ 76.1 76.4 76.3 76.2 76.4 69.3
 5′ 66.2 65.7 66.3 66.3 65.4 67.3
Rha-1′′ 100.3 101.3 101.3 101.7
 2′′ 72.4 72.6 72.9 72.6
 3′′ 72.4 72.5 72.8 72.6
 4′′ 74.3 74.7 74.7 74.5
 5′′ 69.6 69.5 69.4 69.8
 6′′ 19.0 19.0 19.0 19.0
Xyl-1′′ 106.7
 2′′ 75.5
 3′′ 78.3
 4′′ 71.2
 5′′ 67.3
a

Assignments were based on DEPT, 1H-1H COSY, HMQC, and HMBC experiments