Table 3.
Crystallographic Data Collection and Refinement Statistics for Complexes of 17C and 18d with the Wild-Type HIV-1 Proteasea
| 17c | 18d | |
|---|---|---|
| Resolution (Å) | 1.95 | 1.85 |
| Space group | P212121 | P212121 |
| a (Å) | 50.67 | 50.79 |
| b (Å) | 57.86 | 58.25 |
| c (Å) | 61.91 | 62.01 |
| Z | 4 | 4 |
| Rmerge (%) | 10.2 | 8.7 |
| Completeness (%) | 99.7 | 98.4 |
| Total no. of reflections | 91018 | 100852 |
| No. of unique reflections | 13809 | 16073 |
| Rfree (%) | 20.1 | 22.3 |
| Rfactor (%) | 16.5 | 18.0 |
| RMSDa in: | 0.008 | 0.009 |
| Bond lengths (Å) | ||
| RMS Angle (°) | 1.340 | 1.317 |
| Temperature (°C) | −80 | −80 |
| PDB code | 3MXD | 3MXE |
a
RMSD, root mean square deviation; PDB, protein data bank