Table 2. Crystal data and statistics of measurements.
SeMet BamE | BamD | BamC-NT | BamC-CT | |
---|---|---|---|---|
Crystal dimensions (µm) | 270 × 180 | 180 × 40 | 80 × 120 | 370 × 120 |
Space group | C2 | P21 | P1 | P21 |
Unit-cell parameters | ||||
a (Å) | 69.66 | 53.13 | 46.57 | 29.74 |
b (Å) | 96.52 | 33.44 | 46.63 | 59.12 |
c (Å) | 50.49 | 57.80 | 60.20 | 31.06 |
α (°) | 90.00 | 90.00 | 102.70 | 90.00 |
β (°) | 134.06 | 111.44 | 92.86 | 116.37 |
γ (°) | 90.00 | 90.00 | 118.20 | 90.00 |
Resolution limits (Å) | 50–1.8 (1.88–1.80) | 50–1.8 (1.90–1.80) | 50–1.55 (1.65–1.55) | 50–1.28 (1.33–1.28) |
Wavelength (Å) | 0.9789 | 1.0 | 1.06 | 1.07 |
Oscillation angle (°) | 1 | 1 | 1 | 1 |
Observed reflections | 120092 | 111534 | 191281 | 126101 |
Unique reflections | 21093 | 17881 | 56570 | 25297 |
Completeness (%) | 100 (99.8) | 99.4 (97.8) | 95.1 (93.8) | 98.4 (95.6) |
Multiplicity | 5.9 (5.7) | 6 (5.9) | 3.3 (3.1) | 2.5 (1.9) |
〈I〉/〈σ(I)〉 | 25.7 (2.8) | 20.3 (3.9) | 11.15 (2.76) | 10.3 (1.6) |
Rmerge† | 0.07 (0.472) | 0.044 (0.513) | 0.059 (0.443) | 0.065 (0.572) |
R merge = .