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2D CHHC spectra of V6I8-Vpu1–40 (a,b) V6A4-Vpu1–40 (c,d) and A4I8-Vpu1–40 (e,f) in DOPC/DOPG bilayers at various mixing times, with 1D slices at color-coded positions. Green polygons in the 2D spectra indicate regions where intermolecular crosspeaks would appear if intermolecular 13C-13C distances were less than roughly 4 Å. Green arrows in the 1D slices indicate observed intermolecular crosspeaks. 2D CHHC experiments were performed at −50°C.
