Table 3.
Specimen | Determined Analyte | Column | Eluents | Ref. |
---|---|---|---|---|
EBC | 8-iso-PGF2α | Hypercarb Thermo 100 mm × 2.1 mm × 5 μm |
A: acetonitrile B: water (pH 11) isocratic elution A:B (7:3) flow rate 250 μL/min |
[14,17] |
EBC | 8-iso-PGF2α o-Tyr 8-OHdG |
Hypercarb Thermo 100 mm × 2.1 mm × 5 μm | A: aqueous solution of ammonium hydroxide pH 10.5 B: methanol:acetonitrile 60:40 (v/v) + 0.1% of ammonium hydroxide gradient elution |
[85] |
Urine Plasma | 8-iso-PGF2α | Symmetry C8 150 mm × 3.9 mm × 5 μm |
A: 0.1% acetic acid (pH 3) B: acetonitrile isocratic elution A:B (7:3) |
[8] |
Urine | 8-iso-PGF2α | YMC ODS-AQ 50 mm × 2.0 mm × 3 μm |
A: methanol: acetonitrile 5:95(v/v) B: 2 mM ammonium acetate gradient elution flow rate 0.2 mL/min |
[7] |
Urine | 8-iso-PGF2α | Phenomenex Gemini C 18 110 Å, 50mm × 2.0 mm × 3 μm |
A: 0.1% aqueous solution of ammonium hydroxide B: 0.1% ammonium hydroxide in acetonitrile gradient elution |
[9] |
Plasma | 8-iso-15(R)PGF2α 11β-PGF2α 15(R)-PGF2α PGF2α |
Synergi Hydro-RP 250 mm × 2.0mm |
A: water + 0.01% acetic acid B: methanol gradient elution |
[10] |
Urine | 8-iso-PGF2α 8-iso-15(R)-PGF2α 8-iso-PGF2ß PGF2α |
Hypercarb, 5 μm, 1 mm × 150 mm, porous graphitic carbon column | A: water + 0.5% aqueous solution of ammonium hydroxide (pH 9.5) B: acetonitrile:methanol 40:60(v/v) + 0.5% aqueous solution of ammonium hydroxide flow rate 50 μL/min gradient elution |
[6] |