Table 3. Constraints targeting for both PPAP and ATOP and its solutions according to the model.
Run | A:CPEG % | B:Csalt % | C:pH | PPAP % | ATOP nkat | Desirability | ||||
Predicted | Experimental | Importance | Predicted | Experimental | Importance | |||||
1 | 14.33 | 14.27 | 5.77 | 96.08 | 95.24±0.1 | 3 | 11.52 | 10.71±0.1 | 3 | 0.78 |
2 | 15.10 | 14.30 | 5.98 | 97.09 | 96.72±0.4 | 5 | 10.53 | 9.64±0.1 | 3 | 0.79 |
3 | 15.89 | 14.35 | 6.13 | 97.78 | 97.94±1.0 | 5 | 9.64 | 9.18±0.1 | 2 | 0.80 |
4 | 17.63 | 14.42 | 6.30 | 98.73 | 98.72±0.2 | 5 | 7.89 | 7.83±0.1 | 1 | 0.84 |
5 | 14.33 | 14.27 | 5.77 | 96.08 | 96.44±0.1 | 3 | 230.38 | 247.50±2.5 | 3 | 0.78 |
6 | 17.63 | 14.42 | 6.30 | 98.73 | 100.00±0.1 | 5 | 157.79 | 168.55±1.7 | 1 | 0.84 |
Run 1–5: confirmation experiments of small scale (10 g) ATPS; confirmation experiments of large scale (200 g) ATPS.