Table 1. Data-collection statistics.
Crystal form 1 | Crystal form 2 | |
---|---|---|
Crystallization temperature (K) | 293 | 298 |
Wavelength (Å) | 1.5418 | 0.979 |
Space group | P1 | P65 |
Unit-cell parameters (Å, °) | a = 96.9, b = 107.6, c = 131.1, α = 111.3, β = 107.3, γ = 90.7 | a = b = 70.3, c = 399.7 |
Resolution limits (Å) | 50.0–1.9 (2.0–1.9) | 50.0–1.7 (1.8–1.7) |
Completeness (%) | 94.7 (91.8) | 98.3 (89.5) |
Unique reflections | 255620 (36175) | 121422 (16139) |
Multiplicity | 2.1 (2.0) | 5.4 (3.9) |
Rmerge | 0.107 (0.492) | 0.096 (0.485) |
Mean I/σ(I) | 16.7 (1.8) | 10.6 (2.0) |