| Nonius KappaCCD diffractometer | 14652 independent reflections |
| Radiation source: fine-focus sealed tube | 8149 reflections with I > 2σ(I) |
| graphite | Rint = 0.110 |
| Detector resolution: 18 pixels mm-1 | θmax = 27.5°, θmin = 1.8° |
| ω scans at fixed χ = 55° | h = −9→9 |
| Absorption correction: multi-scan (SCALEPACK; Otwinowski & Minor, 1997) | k = −52→52 |
| Tmin = 0.658, Tmax = 0.843 | l = 0→15 |
| 44794 measured reflections |
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