| Rigaku AFC10/Saturn724+ diffractometer | 2481 independent reflections |
| Radiation source: Rotating Anode | 2194 reflections with I > 2σ(I) |
| graphite | Rint = 0.017 |
| Detector resolution: 28.6 pixels mm-1 | θmax = 25.3°, θmin = 3.2° |
| φ and ω scans | h = −8→8 |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | k = −11→11 |
| Tmin = 0.852, Tmax = 0.886 | l = −13→13 |
| 5691 measured reflections |
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