Bruker APEXII DUO CCD diffractometer | 2190 independent reflections |
Radiation source: fine-focus sealed tube | 1895 reflections with I > 2σ(I) |
graphite | Rint = 0.029 |
φ and ω scans | θmax = 32.1°, θmin = 2.2° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −5→5 |
Tmin = 0.841, Tmax = 0.986 | k = −20→20 |
6112 measured reflections | l = −18→18 |