Bruker APEXII CCD area-detector diffractometer | 4506 independent reflections |
Radiation source: sealed tube | 3581 reflections with I > 2σ(I) |
graphite | Rint = 0.029 |
φ and ω scans | θmax = 30.0°, θmin = 1.9° |
Absorption correction: multi-scan (SADABS; Bruker, 2005) | h = −19→19 |
Tmin = 0.965, Tmax = 0.991 | k = −14→12 |
19818 measured reflections | l = −31→31 |