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. 2010 Jul 21;66(Pt 8):o2062. doi: 10.1107/S1600536810028163
Oxford Diffraction Xcalibur diffractometer with an Atlas (Gemini Ultra Cu) detector 2546 independent reflections
Radiation source: X-ray tube 2485 reflections with I > 3σ(I)
mirror Rint = 0.023
Detector resolution: 10.3784 pixels mm-1 θmax = 65.1°, θmin = 4.4°
Rotation method data acquisition using ω scans h = −9→9
Absorption correction: analytical (CrysAlis PRO; Oxford Diffraction, 2009) k = −11→11
Tmin = 0.308, Tmax = 0.631 l = −12→12
11571 measured reflections