Oxford Diffraction Xcalibur diffractometer with an Atlas (Gemini Ultra Cu) detector | 2546 independent reflections |
Radiation source: X-ray tube | 2485 reflections with I > 3σ(I) |
mirror | Rint = 0.023 |
Detector resolution: 10.3784 pixels mm-1 | θmax = 65.1°, θmin = 4.4° |
Rotation method data acquisition using ω scans | h = −9→9 |
Absorption correction: analytical (CrysAlis PRO; Oxford Diffraction, 2009) | k = −11→11 |
Tmin = 0.308, Tmax = 0.631 | l = −12→12 |
11571 measured reflections |