| Bruker SMART 4K CCD area-detector diffractometer | 4713 independent reflections |
| Radiation source: fine-focus sealed tube | 3715 reflections with I > 2σ(I) |
| graphite | Rint = 0.031 |
| φ and ω scans | θmax = 28.3°, θmin = 2.2° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2003) | h = −14→14 |
| Tmin = 0.972, Tmax = 0.991 | k = −13→12 |
| 14116 measured reflections | l = −23→22 |