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. 2010 Oct 31;66(Pt 11):o3004–o3005. doi: 10.1107/S1600536810043564
Refinement on F2 Secondary atom site location: difference Fourier map
Least-squares matrix: full Hydrogen site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.044 H atoms treated by a mixture of independent and constrained refinement
wR(F2) = 0.119 w = 1/[σ2(Fo2) + (0.0537P)2 + 0.0632P] where P = (Fo2 + 2Fc2)/3
S = 1.03 (Δ/σ)max < 0.001
2768 reflections Δρmax = 0.21 e Å3
197 parameters Δρmin = −0.17 e Å3
0 restraints Extinction correction: SHELXTL (Sheldrick, 2008), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
38 constraints Extinction coefficient: 0.0088 (17)
Primary atom site location: structure-invariant direct methods