O1—C1 | 1.360 (3) | C12—H12B | 0.9900 |
O1—C4 | 1.364 (3) | C13—C14 | 1.518 (3) |
O2—C6 | 1.202 (3) | C13—C18 | 1.597 (3) |
O3—C6 | 1.353 (3) | C13—H13 | 1.0000 |
O3—C5 | 1.461 (3) | C14—C15 | 1.510 (3) |
O4—C17 | 1.217 (3) | C15—C16 | 1.550 (3) |
O5—C22 | 1.427 (3) | C15—H15A | 0.9900 |
O5—H5 | 0.84 (1) | C15—H15B | 0.9900 |
O6—C26 | 1.198 (3) | C16—C17 | 1.513 (3) |
O7—C26 | 1.330 (3) | C16—C22 | 1.552 (3) |
O7—C27 | 1.447 (3) | C16—H16 | 1.0000 |
O8—C28 | 1.206 (3) | C17—C18 | 1.533 (3) |
O9—C28 | 1.351 (3) | C18—C19 | 1.540 (3) |
O9—C25 | 1.433 (2) | C18—C20 | 1.576 (3) |
C1—C2 | 1.343 (4) | C19—H19A | 0.9800 |
C1—H1 | 0.9500 | C19—H19B | 0.9800 |
C2—C3 | 1.438 (3) | C19—H19C | 0.9800 |
C2—H2 | 0.9500 | C20—C25 | 1.537 (3) |
C3—C4 | 1.350 (3) | C20—C21 | 1.553 (3) |
C3—C5 | 1.486 (3) | C20—H20 | 1.0000 |
C4—H4 | 0.9500 | C21—C24 | 1.533 (3) |
C5—C9 | 1.548 (3) | C21—C23 | 1.549 (3) |
C5—H5A | 1.0000 | C21—C22 | 1.553 (3) |
C6—C7 | 1.497 (3) | C22—H22 | 1.0000 |
C7—C8 | 1.513 (3) | C23—H23A | 0.9800 |
C7—H7A | 0.9900 | C23—H23B | 0.9800 |
C7—H7B | 0.9900 | C23—H23C | 0.9800 |
C8—C14 | 1.333 (3) | C24—H24A | 0.9800 |
C8—C9 | 1.520 (3) | C24—H24B | 0.9800 |
C9—C11 | 1.538 (3) | C24—H24C | 0.9800 |
C9—C10 | 1.539 (3) | C25—C26 | 1.532 (3) |
C10—H10A | 0.9800 | C25—H25 | 1.0000 |
C10—H10B | 0.9800 | C27—H27A | 0.9800 |
C10—H10C | 0.9800 | C27—H27B | 0.9800 |
C11—C12 | 1.521 (3) | C27—H27C | 0.9800 |
C11—H11A | 0.9900 | C28—C29 | 1.490 (3) |
C11—H11B | 0.9900 | C29—H29A | 0.9800 |
C12—C13 | 1.530 (3) | C29—H29B | 0.9800 |
C12—H12A | 0.9900 | C29—H29C | 0.9800 |
C1—O1—C4 | 105.78 (19) | C17—C16—C22 | 112.35 (18) |
C6—O3—C5 | 119.61 (16) | C15—C16—C22 | 115.07 (18) |
C22—O5—H5 | 104 (2) | C17—C16—H16 | 108.4 |
C26—O7—C27 | 114.67 (18) | C15—C16—H16 | 108.4 |
C28—O9—C25 | 117.71 (17) | C22—C16—H16 | 108.4 |
C2—C1—O1 | 111.4 (2) | O4—C17—C16 | 123.0 (2) |
C2—C1—H1 | 124.3 | O4—C17—C18 | 122.9 (2) |
O1—C1—H1 | 124.3 | C16—C17—C18 | 113.45 (18) |
C1—C2—C3 | 106.0 (2) | C17—C18—C19 | 108.29 (17) |
C1—C2—H2 | 127.0 | C17—C18—C20 | 109.63 (18) |
C3—C2—H2 | 127.0 | C19—C18—C20 | 115.63 (17) |
C4—C3—C2 | 105.6 (2) | C17—C18—C13 | 100.00 (16) |
C4—C3—C5 | 126.4 (2) | C19—C18—C13 | 109.91 (18) |
C2—C3—C5 | 128.0 (2) | C20—C18—C13 | 112.19 (16) |
C3—C4—O1 | 111.2 (2) | C18—C19—H19A | 109.5 |
C3—C4—H4 | 124.4 | C18—C19—H19B | 109.5 |
O1—C4—H4 | 124.4 | H19A—C19—H19B | 109.5 |
O3—C5—C3 | 105.74 (16) | C18—C19—H19C | 109.5 |
O3—C5—C9 | 110.76 (17) | H19A—C19—H19C | 109.5 |
C3—C5—C9 | 115.06 (18) | H19B—C19—H19C | 109.5 |
O3—C5—H5A | 108.4 | C25—C20—C21 | 114.55 (16) |
C3—C5—H5A | 108.4 | C25—C20—C18 | 113.28 (17) |
C9—C5—H5A | 108.4 | C21—C20—C18 | 112.67 (16) |
O2—C6—O3 | 118.5 (2) | C25—C20—H20 | 105.1 |
O2—C6—C7 | 123.5 (2) | C21—C20—H20 | 105.1 |
O3—C6—C7 | 117.99 (19) | C18—C20—H20 | 105.1 |
C6—C7—C8 | 117.74 (19) | C24—C21—C23 | 106.33 (18) |
C6—C7—H7A | 107.9 | C24—C21—C20 | 111.93 (17) |
C8—C7—H7A | 107.9 | C23—C21—C20 | 115.78 (18) |
C6—C7—H7B | 107.9 | C24—C21—C22 | 108.43 (18) |
C8—C7—H7B | 107.9 | C23—C21—C22 | 107.51 (17) |
H7A—C7—H7B | 107.2 | C20—C21—C22 | 106.60 (16) |
C14—C8—C7 | 121.15 (19) | O5—C22—C16 | 108.69 (17) |
C14—C8—C9 | 124.17 (19) | O5—C22—C21 | 112.06 (17) |
C7—C8—C9 | 114.66 (17) | C16—C22—C21 | 112.18 (18) |
C8—C9—C11 | 110.70 (16) | O5—C22—H22 | 107.9 |
C8—C9—C10 | 109.21 (18) | C16—C22—H22 | 107.9 |
C11—C9—C10 | 111.35 (18) | C21—C22—H22 | 107.9 |
C8—C9—C5 | 106.23 (16) | C21—C23—H23A | 109.5 |
C11—C9—C5 | 108.21 (17) | C21—C23—H23B | 109.5 |
C10—C9—C5 | 111.03 (17) | H23A—C23—H23B | 109.5 |
C9—C10—H10A | 109.5 | C21—C23—H23C | 109.5 |
C9—C10—H10B | 109.5 | H23A—C23—H23C | 109.5 |
H10A—C10—H10B | 109.5 | H23B—C23—H23C | 109.5 |
C9—C10—H10C | 109.5 | C21—C24—H24A | 109.5 |
H10A—C10—H10C | 109.5 | C21—C24—H24B | 109.5 |
H10B—C10—H10C | 109.5 | H24A—C24—H24B | 109.5 |
C12—C11—C9 | 112.46 (17) | C21—C24—H24C | 109.5 |
C12—C11—H11A | 109.1 | H24A—C24—H24C | 109.5 |
C9—C11—H11A | 109.1 | H24B—C24—H24C | 109.5 |
C12—C11—H11B | 109.1 | O9—C25—C26 | 111.32 (17) |
C9—C11—H11B | 109.1 | O9—C25—C20 | 109.29 (16) |
H11A—C11—H11B | 107.8 | C26—C25—C20 | 112.31 (17) |
C11—C12—C13 | 114.02 (17) | O9—C25—H25 | 107.9 |
C11—C12—H12A | 108.7 | C26—C25—H25 | 107.9 |
C13—C12—H12A | 108.7 | C20—C25—H25 | 107.9 |
C11—C12—H12B | 108.7 | O6—C26—O7 | 124.9 (2) |
C13—C12—H12B | 108.7 | O6—C26—C25 | 122.11 (19) |
H12A—C12—H12B | 107.6 | O7—C26—C25 | 112.95 (18) |
C14—C13—C12 | 112.65 (17) | O7—C27—H27A | 109.5 |
C14—C13—C18 | 108.77 (17) | O7—C27—H27B | 109.5 |
C12—C13—C18 | 117.01 (18) | H27A—C27—H27B | 109.5 |
C14—C13—H13 | 105.9 | O7—C27—H27C | 109.5 |
C12—C13—H13 | 105.9 | H27A—C27—H27C | 109.5 |
C18—C13—H13 | 105.9 | H27B—C27—H27C | 109.5 |
C8—C14—C15 | 122.6 (2) | O8—C28—O9 | 122.2 (2) |
C8—C14—C13 | 123.70 (19) | O8—C28—C29 | 126.9 (2) |
C15—C14—C13 | 113.74 (17) | O9—C28—C29 | 110.79 (19) |
C14—C15—C16 | 113.10 (17) | C28—C29—H29A | 109.5 |
C14—C15—H15A | 109.0 | C28—C29—H29B | 109.5 |
C16—C15—H15A | 109.0 | H29A—C29—H29B | 109.5 |
C14—C15—H15B | 109.0 | C28—C29—H29C | 109.5 |
C16—C15—H15B | 109.0 | H29A—C29—H29C | 109.5 |
H15A—C15—H15B | 107.8 | H29B—C29—H29C | 109.5 |
C17—C16—C15 | 103.94 (19) | ||
C4—O1—C1—C2 | 0.9 (3) | C15—C16—C17—C18 | −68.0 (2) |
O1—C1—C2—C3 | −0.4 (3) | C22—C16—C17—C18 | 57.1 (2) |
C1—C2—C3—C4 | −0.3 (3) | O4—C17—C18—C19 | 17.1 (3) |
C1—C2—C3—C5 | 177.9 (2) | C16—C17—C18—C19 | −171.89 (18) |
C2—C3—C4—O1 | 0.9 (3) | O4—C17—C18—C20 | 144.1 (2) |
C5—C3—C4—O1 | −177.3 (2) | C16—C17—C18—C20 | −44.9 (2) |
C1—O1—C4—C3 | −1.1 (3) | O4—C17—C18—C13 | −97.9 (2) |
C6—O3—C5—C3 | −166.70 (18) | C16—C17—C18—C13 | 73.1 (2) |
C6—O3—C5—C9 | −41.4 (2) | C14—C13—C18—C17 | −62.5 (2) |
C4—C3—C5—O3 | −140.9 (2) | C12—C13—C18—C17 | 168.46 (18) |
C2—C3—C5—O3 | 41.3 (3) | C14—C13—C18—C19 | −176.26 (17) |
C4—C3—C5—C9 | 96.5 (3) | C12—C13—C18—C19 | 54.7 (2) |
C2—C3—C5—C9 | −81.3 (3) | C14—C13—C18—C20 | 53.6 (2) |
C5—O3—C6—O2 | 177.6 (2) | C12—C13—C18—C20 | −75.4 (2) |
C5—O3—C6—C7 | −5.1 (3) | C17—C18—C20—C25 | −147.54 (17) |
O2—C6—C7—C8 | −155.4 (2) | C19—C18—C20—C25 | −24.8 (2) |
O3—C6—C7—C8 | 27.5 (3) | C13—C18—C20—C25 | 102.3 (2) |
C6—C7—C8—C14 | −179.1 (2) | C17—C18—C20—C21 | −15.5 (2) |
C6—C7—C8—C9 | −0.7 (3) | C19—C18—C20—C21 | 107.2 (2) |
C14—C8—C9—C11 | 19.3 (3) | C13—C18—C20—C21 | −125.63 (18) |
C7—C8—C9—C11 | −159.00 (18) | C25—C20—C21—C24 | −46.3 (2) |
C14—C8—C9—C10 | −103.6 (2) | C18—C20—C21—C24 | −177.77 (17) |
C7—C8—C9—C10 | 78.1 (2) | C25—C20—C21—C23 | 75.7 (2) |
C14—C8—C9—C5 | 136.6 (2) | C18—C20—C21—C23 | −55.7 (2) |
C7—C8—C9—C5 | −41.7 (2) | C25—C20—C21—C22 | −164.74 (17) |
O3—C5—C9—C8 | 63.6 (2) | C18—C20—C21—C22 | 63.8 (2) |
C3—C5—C9—C8 | −176.52 (18) | C17—C16—C22—O5 | −129.80 (18) |
O3—C5—C9—C11 | −177.45 (16) | C15—C16—C22—O5 | −11.1 (2) |
C3—C5—C9—C11 | −57.6 (2) | C17—C16—C22—C21 | −5.3 (2) |
O3—C5—C9—C10 | −55.0 (2) | C15—C16—C22—C21 | 113.3 (2) |
C3—C5—C9—C10 | 64.9 (2) | C24—C21—C22—O5 | −49.9 (2) |
C8—C9—C11—C12 | −45.1 (2) | C23—C21—C22—O5 | −164.50 (18) |
C10—C9—C11—C12 | 76.6 (2) | C20—C21—C22—O5 | 70.7 (2) |
C5—C9—C11—C12 | −161.11 (17) | C24—C21—C22—C16 | −172.51 (17) |
C9—C11—C12—C13 | 55.3 (2) | C23—C21—C22—C16 | 72.9 (2) |
C11—C12—C13—C14 | −35.6 (3) | C20—C21—C22—C16 | −51.8 (2) |
C11—C12—C13—C18 | 91.5 (2) | C28—O9—C25—C26 | 90.9 (2) |
C7—C8—C14—C15 | −2.3 (3) | C28—O9—C25—C20 | −144.50 (18) |
C9—C8—C14—C15 | 179.45 (19) | C21—C20—C25—O9 | −47.2 (2) |
C7—C8—C14—C13 | 177.06 (19) | C18—C20—C25—O9 | 84.0 (2) |
C9—C8—C14—C13 | −1.2 (3) | C21—C20—C25—C26 | 76.9 (2) |
C12—C13—C14—C8 | 8.9 (3) | C18—C20—C25—C26 | −151.96 (17) |
C18—C13—C14—C8 | −122.5 (2) | C27—O7—C26—O6 | −3.3 (4) |
C12—C13—C14—C15 | −171.68 (18) | C27—O7—C26—C25 | 179.2 (2) |
C18—C13—C14—C15 | 56.9 (2) | O9—C25—C26—O6 | 174.3 (2) |
C8—C14—C15—C16 | 127.9 (2) | C20—C25—C26—O6 | 51.4 (3) |
C13—C14—C15—C16 | −51.6 (3) | O9—C25—C26—O7 | −8.1 (3) |
C14—C15—C16—C17 | 52.2 (2) | C20—C25—C26—O7 | −131.01 (19) |
C14—C15—C16—C22 | −71.1 (2) | C25—O9—C28—O8 | −1.2 (3) |
C15—C16—C17—O4 | 103.1 (2) | C25—O9—C28—C29 | 177.21 (17) |
C22—C16—C17—O4 | −131.9 (2) |