O1—C1 | 1.355 (2) | C11—C14 | 1.531 (3) |
O1—H1 | 0.866 (10) | C11—C13 | 1.537 (3) |
O2—C22 | 1.207 (2) | C11—C12 | 1.537 (3) |
O3—C22 | 1.346 (2) | C12—H12A | 0.9800 |
O3—C23 | 1.450 (2) | C12—H12B | 0.9800 |
N1—C15 | 1.273 (3) | C12—H12C | 0.9800 |
N1—C16 | 1.428 (3) | C13—H13A | 0.9800 |
C1—C6 | 1.406 (3) | C13—H13B | 0.9800 |
C1—C2 | 1.410 (3) | C13—H13C | 0.9800 |
C2—C3 | 1.397 (3) | C14—H14A | 0.9800 |
C2—C8 | 1.535 (3) | C14—H14B | 0.9800 |
C3—C4 | 1.402 (3) | C14—H14C | 0.9800 |
C3—H3 | 0.9500 | C15—H15 | 0.9500 |
C4—C5 | 1.389 (3) | C16—C17 | 1.381 (3) |
C4—C11 | 1.529 (3) | C16—C21 | 1.399 (3) |
C5—C6 | 1.393 (3) | C17—C18 | 1.379 (3) |
C5—H5 | 0.9500 | C17—H17 | 0.9500 |
C6—C15 | 1.465 (3) | C18—C19 | 1.395 (3) |
C7—C8 | 1.540 (3) | C18—H18 | 0.9500 |
C7—H7A | 0.9800 | C19—C20 | 1.389 (3) |
C7—H7B | 0.9800 | C19—C22 | 1.488 (3) |
C7—H7C | 0.9800 | C20—C21 | 1.387 (3) |
C8—C10 | 1.534 (3) | C20—H20 | 0.9500 |
C8—C9 | 1.539 (3) | C21—H21 | 0.9500 |
C9—H9A | 0.9800 | C23—C24 | 1.494 (3) |
C9—H9B | 0.9800 | C23—H23A | 0.9900 |
C9—H9C | 0.9800 | C23—H23B | 0.9900 |
C10—H10A | 0.9800 | C24—H24A | 0.9800 |
C10—H10B | 0.9800 | C24—H24B | 0.9800 |
C10—H10C | 0.9800 | C24—H24C | 0.9800 |
C1—O1—H1 | 106 (2) | H12A—C12—H12B | 109.5 |
C22—O3—C23 | 114.99 (16) | C11—C12—H12C | 109.5 |
C15—N1—C16 | 118.83 (18) | H12A—C12—H12C | 109.5 |
O1—C1—C6 | 119.20 (18) | H12B—C12—H12C | 109.5 |
O1—C1—C2 | 120.37 (18) | C11—C13—H13A | 109.5 |
C6—C1—C2 | 120.43 (18) | C11—C13—H13B | 109.5 |
C3—C2—C1 | 116.73 (18) | H13A—C13—H13B | 109.5 |
C3—C2—C8 | 121.24 (17) | C11—C13—H13C | 109.5 |
C1—C2—C8 | 121.96 (18) | H13A—C13—H13C | 109.5 |
C2—C3—C4 | 124.26 (18) | H13B—C13—H13C | 109.5 |
C2—C3—H3 | 117.9 | C11—C14—H14A | 109.5 |
C4—C3—H3 | 117.9 | C11—C14—H14B | 109.5 |
C5—C4—C3 | 116.83 (18) | H14A—C14—H14B | 109.5 |
C5—C4—C11 | 120.03 (17) | C11—C14—H14C | 109.5 |
C3—C4—C11 | 123.12 (17) | H14A—C14—H14C | 109.5 |
C4—C5—C6 | 121.49 (19) | H14B—C14—H14C | 109.5 |
C4—C5—H5 | 119.3 | N1—C15—C6 | 122.09 (19) |
C6—C5—H5 | 119.3 | N1—C15—H15 | 119.0 |
C5—C6—C1 | 120.03 (18) | C6—C15—H15 | 119.0 |
C5—C6—C15 | 117.32 (18) | C17—C16—C21 | 119.51 (19) |
C1—C6—C15 | 122.63 (19) | C17—C16—N1 | 117.79 (19) |
C8—C7—H7A | 109.5 | C21—C16—N1 | 122.64 (19) |
C8—C7—H7B | 109.5 | C18—C17—C16 | 120.3 (2) |
H7A—C7—H7B | 109.5 | C18—C17—H17 | 119.8 |
C8—C7—H7C | 109.5 | C16—C17—H17 | 119.8 |
H7A—C7—H7C | 109.5 | C17—C18—C19 | 120.5 (2) |
H7B—C7—H7C | 109.5 | C17—C18—H18 | 119.7 |
C10—C8—C2 | 112.00 (17) | C19—C18—H18 | 119.7 |
C10—C8—C7 | 107.87 (18) | C20—C19—C18 | 119.40 (18) |
C2—C8—C7 | 108.92 (17) | C20—C19—C22 | 122.69 (19) |
C10—C8—C9 | 106.89 (17) | C18—C19—C22 | 117.87 (18) |
C2—C8—C9 | 111.03 (17) | C21—C20—C19 | 120.0 (2) |
C7—C8—C9 | 110.07 (18) | C21—C20—H20 | 120.0 |
C8—C9—H9A | 109.5 | C19—C20—H20 | 120.0 |
C8—C9—H9B | 109.5 | C20—C21—C16 | 120.18 (19) |
H9A—C9—H9B | 109.5 | C20—C21—H21 | 119.9 |
C8—C9—H9C | 109.5 | C16—C21—H21 | 119.9 |
H9A—C9—H9C | 109.5 | O2—C22—O3 | 123.23 (18) |
H9B—C9—H9C | 109.5 | O2—C22—C19 | 124.17 (19) |
C8—C10—H10A | 109.5 | O3—C22—C19 | 112.57 (17) |
C8—C10—H10B | 109.5 | O3—C23—C24 | 107.99 (17) |
H10A—C10—H10B | 109.5 | O3—C23—H23A | 110.1 |
C8—C10—H10C | 109.5 | C24—C23—H23A | 110.1 |
H10A—C10—H10C | 109.5 | O3—C23—H23B | 110.1 |
H10B—C10—H10C | 109.5 | C24—C23—H23B | 110.1 |
C4—C11—C14 | 112.55 (16) | H23A—C23—H23B | 108.4 |
C4—C11—C13 | 108.92 (16) | C23—C24—H24A | 109.5 |
C14—C11—C13 | 108.30 (16) | C23—C24—H24B | 109.5 |
C4—C11—C12 | 109.85 (16) | H24A—C24—H24B | 109.5 |
C14—C11—C12 | 107.53 (17) | C23—C24—H24C | 109.5 |
C13—C11—C12 | 109.64 (17) | H24A—C24—H24C | 109.5 |
C11—C12—H12A | 109.5 | H24B—C24—H24C | 109.5 |
C11—C12—H12B | 109.5 | ||
O1—C1—C2—C3 | −175.11 (17) | C3—C4—C11—C13 | −122.2 (2) |
C6—C1—C2—C3 | 4.6 (3) | C5—C4—C11—C12 | −64.1 (2) |
O1—C1—C2—C8 | 1.8 (3) | C3—C4—C11—C12 | 117.6 (2) |
C6—C1—C2—C8 | −178.52 (18) | C16—N1—C15—C6 | 178.21 (17) |
C1—C2—C3—C4 | −1.5 (3) | C5—C6—C15—N1 | −174.29 (19) |
C8—C2—C3—C4 | −178.36 (18) | C1—C6—C15—N1 | 4.0 (3) |
C2—C3—C4—C5 | −2.7 (3) | C15—N1—C16—C17 | 151.3 (2) |
C2—C3—C4—C11 | 175.58 (19) | C15—N1—C16—C21 | −31.4 (3) |
C3—C4—C5—C6 | 3.9 (3) | C21—C16—C17—C18 | 3.2 (3) |
C11—C4—C5—C6 | −174.44 (18) | N1—C16—C17—C18 | −179.46 (18) |
C4—C5—C6—C1 | −0.9 (3) | C16—C17—C18—C19 | −0.4 (3) |
C4—C5—C6—C15 | 177.43 (18) | C17—C18—C19—C20 | −2.2 (3) |
O1—C1—C6—C5 | 176.18 (18) | C17—C18—C19—C22 | 175.61 (19) |
C2—C1—C6—C5 | −3.5 (3) | C18—C19—C20—C21 | 2.0 (3) |
O1—C1—C6—C15 | −2.1 (3) | C22—C19—C20—C21 | −175.68 (18) |
C2—C1—C6—C15 | 178.18 (18) | C19—C20—C21—C16 | 0.8 (3) |
C3—C2—C8—C10 | −9.4 (3) | C17—C16—C21—C20 | −3.4 (3) |
C1—C2—C8—C10 | 173.86 (19) | N1—C16—C21—C20 | 179.43 (18) |
C3—C2—C8—C7 | 109.8 (2) | C23—O3—C22—O2 | 0.8 (3) |
C1—C2—C8—C7 | −66.9 (2) | C23—O3—C22—C19 | 178.95 (17) |
C3—C2—C8—C9 | −128.8 (2) | C20—C19—C22—O2 | 177.1 (2) |
C1—C2—C8—C9 | 54.5 (2) | C18—C19—C22—O2 | −0.6 (3) |
C5—C4—C11—C14 | 176.14 (18) | C20—C19—C22—O3 | −1.0 (3) |
C3—C4—C11—C14 | −2.1 (3) | C18—C19—C22—O3 | −178.74 (18) |
C5—C4—C11—C13 | 56.0 (2) | C22—O3—C23—C24 | −173.52 (17) |