| Bruker SMART APEX diffractometer | 1162 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.089 |
| graphite | θmax = 25.0°, θmin = 1.8° |
| ω scans | h = −5→5 |
| 10723 measured reflections | k = −14→14 |
| 1449 independent reflections | l = −26→25 |
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