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. 2010 Oct 23;66(Pt 11):o2886–o2887. doi: 10.1107/S1600536810041656
Nonius KappaCCD diffractometer 1867 independent reflections
Radiation source: Enraf Nonius FR591 rotating anode 1628 reflections with I > 2σ(I)
10 cm confocal mirrors Rint = 0.044
Detector resolution: 9.091 pixels mm-1 θmax = 27.5°, θmin = 3.0°
φ and ω scans h = −5→5
Absorption correction: multi-scan (SADABS; Sheldrick, 2007) k = −13→13
Tmin = 0.631, Tmax = 0.746 l = −22→22
16245 measured reflections