| Nonius KappaCCD diffractometer | 1867 independent reflections |
| Radiation source: Enraf Nonius FR591 rotating anode | 1628 reflections with I > 2σ(I) |
| 10 cm confocal mirrors | Rint = 0.044 |
| Detector resolution: 9.091 pixels mm-1 | θmax = 27.5°, θmin = 3.0° |
| φ and ω scans | h = −5→5 |
| Absorption correction: multi-scan (SADABS; Sheldrick, 2007) | k = −13→13 |
| Tmin = 0.631, Tmax = 0.746 | l = −22→22 |
| 16245 measured reflections |