| Bruker APEXII CCD diffractometer | 2264 independent reflections |
| Radiation source: fine-focus sealed tube | 2151 reflections with I > 2σ(I) |
| graphite | Rint = 0.035 |
| φ and ω scans | θmax = 30.5°, θmin = 2.4° |
| Absorption correction: multi-scan (SADABS; Bruker, 1998) | h = −48→44 |
| Tmin = 0.945, Tmax = 0.966 | k = −10→10 |
| 7265 measured reflections | l = −9→7 |