| Bruker SMART APEX diffractometer | 2989 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.027 |
| graphite | θmax = 27.5°, θmin = 2.0° |
| ω scans | h = −16→15 |
| 13992 measured reflections | k = −10→10 |
| 3464 independent reflections | l = −18→18 |
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