| Bruker APEX CCD area-detector diffractometer | 5044 independent reflections |
| Radiation source: fine-focus sealed tube | 4821 reflections with I > 2σ(I) |
| graphite | Rint = 0.023 |
| φ and ω scans | θmax = 28.1°, θmin = 2.8° |
| Absorption correction: multi-scan (SADABS; Bruker, 1998) | h = −10→10 |
| Tmin = 0.804, Tmax = 0.885 | k = −13→13 |
| 10484 measured reflections | l = −18→18 |