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Synthesis of DFMP inhibitor 3. Reagents and conditions: (a) bis(neoglycolato)diboron, K3PO4, SPhos, Pd2(dba)3·CHCl3, toluene, 100 °C; (b) NaI, chloramine-T, 50% aq THF; (c) diethyl(bromodifluoromethyl)phosphonate, Zn°, CuBr, DMA; (c) TMSI, CHCl3.
