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. 2010 Dec 23;5(12):e15367. doi: 10.1371/journal.pone.0015367

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Globisch et al.

This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are properly credited.

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a) CO, PPh₃, Pd₂(dba)₃·CHCl₃, Bu₃SnH, 97%, with Bu₃SnD 49%, b) HF pyridine, 75%, c) NaBD₄, CeCl₃·7H₂O, 21%, d) TBAF, 51%, e) CO, TMS-Et-OH, DIPEA, Pd₂Cl₂(MeCN)₂, 52%, f) TBAF, 69%, g) Reference [11] h) HF·pyridine, 70%. All reactions could also be carried out in a protective group free manner but resulted in reduced yields and tedious workups (see Figure S2 for details).