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. Author manuscript; available in PMC: 2011 Dec 23.
Published in final edited form as: J Med Chem. 2010 Nov 24;53(24):8688–8699. doi: 10.1021/jm1011066

Table 3.

NMR Spectroscopic Data for 2-Bromo-1-hydroxyphenazine (1) in CDCl3 at 500 MHz (Assignments made by analysis of 2D NMR Data).

C/H # δH (J Hz) δC COSY HMBC
1 149.3 C
2 103.9 C
3 7.83 d (8.6) 135.5 CH H-4 C-1, C-2, C-4a
4 7.63 d (8.6) 121.3 CH H-3 C-2, C-3, C-10a
4a 100.0 C
5
5a 141.7 C
6 8.18 d (8.4) 129.1 CH H-7. H-8 C-8, C-9a
7 7.82 m 131.6 CH H-6, H-8, H-9 C-7, C-
8 7.82 m 131.6 CH H-6, H-7, H-9 C-7, C-9a
9 8.20 d (8.4) 129.5 CH H-7, H-8 C-8, C-5a
9a 141.7 C
10
10a 134.2 C
1-OH 8.52 br s