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. Author manuscript; available in PMC: 2012 Mar 1.
Published in final edited form as: J Inorg Biochem. 2010 Sep 22;105(3):467–475. doi: 10.1016/j.jinorgbio.2010.08.011

Scheme 1.

Scheme 1

Synthesis of 2-((6-methoxyquinolin-4-yl)methyl)-8-vinylquinuclidine (2, DHQN): i). TsCl, Et3N, CH2Cl2, 9 h, 0°C to rt, 34 % yield; ii). LiAlH4, THF, 12 h, rt, 27 % yield.