Bruker APEXII CCD area-detector diffractometer | 2625 independent reflections |
Radiation source: fine-focus sealed tube | 1940 reflections with I > 2σ(I) |
graphite | Rint = 0.023 |
φ and ω scans | θmax = 27.5°, θmin = 2.4° |
Absorption correction: multi-scan (SADABS; Bruker, 2005) | h = −18→17 |
Tmin = 0.762, Tmax = 0.951 | k = −10→13 |
8253 measured reflections | l = −8→10 |