| Bruker APEXII area-detector diffractometer | 3927 independent reflections |
| Radiation source: fine-focus sealed tube | 3106 reflections with I > 2σ(I) |
| graphite | Rint = 0.028 |
| ω scans | θmax = 27.7°, θmin = 2.3° |
| Absorption correction: multi-scan (SADABS; Sheldrick, 1996) | h = −12→12 |
| Tmin = 0.935, Tmax = 0.978 | k = −13→13 |
| 24834 measured reflections | l = −23→23 |