Bruker SMART 1000 CCD diffractometer | 5726 independent reflections |
Radiation source: fine-focus sealed tube | 3020 reflections with I > 2σ(I) |
graphite | Rint = 0.0000 |
ω scans | θmax = 27.0°, θmin = 1.5° |
Absorption correction: multi-scan (SADABS; Bruker, 2001) | h = −16→15 |
Tmin = 0.982, Tmax = 0.985 | k = 0→17 |
5726 measured reflections | l = 0→21 |