Bruker APEXII DUO CCD area-detector diffractometer | 4135 independent reflections |
Radiation source: fine-focus sealed tube | 3176 reflections with I > 2σ(I) |
graphite | Rint = 0.054 |
φ and ω scans | θmax = 32.6°, θmin = 2.2° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −14→14 |
Tmin = 0.968, Tmax = 0.984 | k = −7→7 |
27219 measured reflections | l = −36→37 |