| Bruker Kappa APEXII CCD diffractometer | 8912 independent reflections |
| Radiation source: fine-focus sealed tube | 4643 reflections with I > 2σ(I) |
| graphite | Rint = 0.092 |
| Detector resolution: 8.3 pixels mm-1 | θmax = 25.1°, θmin = 1.2° |
| ω scans | h = −12→11 |
| Absorption correction: multi-scan (SADABS; Bruker, 2005) | k = −18→18 |
| Tmin = 0.982, Tmax = 0.988 | l = −20→20 |
| 34716 measured reflections |