Table 2. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| O8—H8⋯O14 | 0.82 | 1.67 | 2.491 (4) | 174 |
| O13—H13A⋯O6i | 0.85 (2) | 2.29 (2) | 2.917 (4) | 131 (3) |
| O13—H13B⋯O4ii | 0.85 (3) | 2.09 (2) | 2.926 (4) | 168 (3) |
| O14—H14A⋯O4ii | 0.85 (2) | 1.80 (2) | 2.645 (4) | 174 (3) |
| O14—H14B⋯O15 | 0.85 (3) | 1.98 (4) | 2.658 (6) | 136 (4) |
| O9—H9⋯O2iii | 0.82 | 1.70 | 2.520 (3) | 173 |
| O11—H11A⋯O13iv | 0.82 | 1.84 | 2.634 (4) | 163 |
| N4—H4A⋯O6i | 0.89 | 2.06 | 2.935 (3) | 167 |
| N4—H4A⋯O5i | 0.89 | 2.53 | 2.993 (3) | 113 |
| N4—H4A⋯O11v | 0.89 | 2.58 | 3.011 (3) | 110 |
| N4—H4B⋯O10vi | 0.89 | 2.05 | 2.834 (3) | 146 |
| N4—H4C⋯O9v | 0.89 | 2.41 | 2.964 (3) | 121 |
| N5—H5A⋯O1vii | 0.99 (3) | 2.12 (3) | 3.060 (3) | 158 (3) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
.