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. 2009 Dec 5;17(Pt 1):107–118. doi: 10.1107/S0909049509041168

Table 2. X-ray data-collection statistics for IREM-1 IgV-like domain.

Values in parentheses are for the highest-resolution shell.

Wavelength (Å) 0.873
Temperature (K) 100
Space group P3121
Unit-cell parameters (Å) a = b = 54.23, c = 72.01
 
  Merged Data set 1 Data set 2 Data set 3 Data set 4
No. of frames 90 20 33 30 7
Resolution (Å) 19.67–2.60 19.67–2.60 19.67–2.60 19.67–2.61 19.67–2.61
No. of observations 19419 4506 7453 6570 1479
Unique reflections 3936 2686 2783 2984 1265
Data completeness (%) 97.7 (95.7) 65.1 (65.3) 68.7 (66.9) 76.9 (80.6)§ 31.3 (29.4)§
I/σ(I)〉 9.67 (3.2) 6.02 (2.9) 7.04 (2.9) 7.34 (3.1)§ 3.96 (2.2)§
Rmerge (%) 14.2 (38.8) 12.5 (25.4) 19.3 (47.6) 16.1 (42.1)§ 19.1 (38.6)§
Molecules per asymmetric unit 1
Crystal solvent content (%) 37.27

Higher-resolution shell 2.60–2.70 Å.

Higher-resolution shell 2.60–2.76 Å.

§

Higher-resolution shell 2.61–2.76 Å.

R merge = ΣhΣi|I hi − 〈I h〉|/ΣhΣi I hi, where I hi is the intensity of an individual reflection.