TABLE 1.
| ||||
---|---|---|---|---|
entry | substrate | product | isolated yield (%) | |
1 | 1a | 96b | ||
2 | 1b | 99 | ||
3 | 1c | 97 | ||
4 | 1d | 98 | ||
5 | 1e | 93 | ||
6 | 1f | 97 | ||
7 | 1g | 95 | ||
8 | 1h | 94 | ||
9 | 1i | 99 | ||
10 | 1j | 97 |
All reactions were carried out using 1 mmol of aryltrifluoroborate and Oxone (5 mL, 0.2 M in H2O) in 5 mL of acetone for 2 min at rt.
55 mmol scale.