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. 2011 Jan 24;6(1):e14575. doi: 10.1371/journal.pone.0014575

Table 1. LC/TOF-MS data of phenolic compounds.

No. tR [min] Compound m/z [M-H]- m/z of in-source fragment ions
1 6.91 Gallic acid 169.0141 125.0232
2 14.86 Procyanidin B1 577.1332 407.0693, 289.0701, 245.0778
3* 15.37 Procyanidin dimer 577.1282 407.0728, 289.0678, 245.0655
4 15.95 (+)-Catechin 289.0716 245.0789, 203.0715
5* 16.72 Procyanidin trimer 865.1968 713.1505, 695.1157, 577.1189, 407.0724, 289.0743, 245.0564
6* 17.35 Procyanidin dimer 577.1344 407.0749, 289.0713, 245.0683
7 17.91 Procyanidin B2 577.1341 407.0733, 289.0683, 245.0772
8* 18.63 Procyanidin dimer 577.1326 407.0753, 289.0712, 245.0707
9 19.13 (−)-Epicatechin 289.0706 245.0792, 203.0666
10* 20.51 Procyanidin trimer 865.1982 713.1497, 695.1391, 577.1267, 407.0772, 289.0677, 245.0544
11* 21.26 Procyanidin dimer gallate 729.1464 577.1216, 407.0760, 289.0700, 245.0597
12* 21.31 Procyanidin tetramer 1153.2642 1001.2333, 983.2046, 865.1931, 577.1223, 407.0764, 289.0703, 245.0601
13* 24.26 Epicatechin-3-O-gallate 441.0824 289.0706, 245.0644, 169.0143
14* 24.85 Procyanidin dimer 577.1276 407.0717, 289.0692, 245.0713

Asterisk indicates those only detected in KOS GSE.