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ENDOR spectra of b-SO: νmw = 9.4196 GHz; B0 = 3385 G (at gZ). Left panel: 1H Davies ENDOR in H2O (solid line) and D2O (dashed line) buffers. Comparison of these two spectra shows that the external shoulders belong to exchangeable protons with hfi up to 7 MHz. Right panel: 2H Mims ENDOR in D2O buffer. The Spectrum presents only exchangeable deuterons. The maximal hfi (rescaled to protons) is ~7–7.5 MHz, in agreement with the spectra shown in the left panel.
