Table 2.
entry | alkene | product | yieldb |
---|---|---|---|
1 | 75% | ||
2 | 84% | ||
3 | 53% | ||
4 | 85% | ||
5 | 80% | ||
6 | 98% | ||
7 | 81% | ||
8 | 46% |
All reactions were performed by heating the oxime (1 equiv), alkene (3 equiv), [Cp*RhCl2]2 (5 mol %), AgSbF6 (20 mol %), Cu(OAc)2 (2.1 equiv), and THF (0.1 M) in a sealed vial for 20 h at 75 °C.
Isolated yields after purification by chromatography are reported.