Table 1. Data-collection and processing statistics.
Values in parentheses are for the highest resolution shell.
| No. of crystals | 1 |
| Beamline | X6A |
| Wavelength (Å) | 0.95370 |
| Detector | ADSC Q270 CCD [270 × 270 mm] |
| Crystal-to-detector distance (mm) | 150 |
| Rotation range per image (°) | 0.5 |
| Total rotation range (°) | 245 |
| Exposure time per image (s) | 45 |
| Resolution range (Å) | 30–1.65 |
| Space group | P212121 |
| Unit-cell parameters (Å) | a = 28.1, b = 60.7, c = 104.8 |
| Mosaicity (°) | 1.6 |
| Total No. of measured intensities | 22132 |
| Unique reflections | 796328 |
| Multiplicity | 9.8 |
| Mean I/σ(I) | 33.0 (2.6) |
| Completeness (%) | 99.7 (99.6) |
| Rmerge (%)† | 6.8 |
| Rmeas or Rr.i.m. (%) | 20.7 |
†
R
merge = 
, where Ii(hkl) is the ith observation of reflection hkl and 〈I(hkl)〉 is the weighted average intensity for all observations i of reflection hkl (Diederichs & Karplus, 1997 ▶).