Table 1.
Position | δc | δH | H-H COSY | HMBC |
---|---|---|---|---|
1 | 164.1 | |||
2 | 107.8 | 6.51 (H, d, 2.4) | 4 | 1, 3, 4, 9a |
3 | 165.4 | |||
4 | 109.0 | 7.03 (H, d, 2.4) | 2 | 4, 10 |
4a | 134.4 | |||
5 | 101.2 | 6.98 (H, s) | 7, 8, 8a, 10 | |
6 | 159.1 | |||
7 | 117.1 | |||
8 | 165.0 | |||
8a | 110.5 | |||
9 | 188.4 | |||
9a | 108.0 | |||
10 | 180.4 | |||
10a | 135.2 | |||
11 | 112.8 | 6.60 (H, d, 5.5) | 12 | 7, 8, 12, 13, 14 |
12 | 53.2 | 3.91 (d, 5.5) | 11 | 6, 7, 8, 11, 13, 14 |
13 | 72.7 | 4.44 (d, 1.8) | 14 | 7, 11, 14 |
14 | 74.8 | 3.59 (H, dd, 2.3,10.1), 3.91 (H, d, 10.1) | 13 | 11, 12, 13 |