Table 2.
Data collection, Structure Determination and Refinement Statistics of IL1β-S1.
| Data Collection of IL1β-S1 | |
|---|---|
| Space group and unit cell | P6322; a = b = 120.6 A, c = 74.9Å |
| Wavelength (Å) | 0.95000 |
| Resolution limits (Å) (highest resolution shell) no. of reflections | 50-2.10 (2.18-2.10) |
| Measured | 294259 |
| Unique | 19092 |
| Completeness (%) | |
| All data (highest resolution shell) | 99.0 |
| Rsyma (on I) (highest resolution shell) | 0.075 (0.274) |
| [I/σ(I)] | |
| all data (highest resolution shell) | 21.2 (3.9) |
| | |
| Structure Determination | |
| <m>SOLVE | 0.25 |
| <m>RESOLVE | 0.64 |
| | |
| Refinement | |
| Resolution (Å) | 50-2.1 |
| R factor | 0.192 |
| R free | 0.224 |
| Reflections in test set | 3225 |
| non-hydrogen atoms | 1486 |
| RMS deviations | |
| Bond lengths (Å) | 0.008 |
| Angles (°) | 1.16 |
| Average B factor (Å2) (all atoms) | 31.0 |
Rsym = Σ|Iobs – <I>|/ΣIobs