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. Author manuscript; available in PMC: 2012 May 10.
Published in final edited form as: J Am Chem Soc. 2010 Nov 11;132(48):17118–17129. doi: 10.1021/ja1045428

Figure 11.

Figure 11

4.2 K Mössbauer spectrum obtained after adding ~6 equivalents pyridinium triflate at −40 °C to 1.3 mM 2. 38% of the iron belongs to complex 5 and 47% to 3; the remainder of the iron belongs to broad and unresolved FeIII species.