| Stoe IPDS 2 CCD diffractometer | 4206 independent reflections |
| Radiation source: fine-focus sealed tube | 1375 reflections with I > 2σ(I) |
| plane graphite | Rint = 0.135 |
| rotation method scans | θmax = 25.0°, θmin = 1.6° |
| Absorption correction: integration (X-RED32; Stoe & Cie, 2002) | h = −8→7 |
| Tmin = 0.797, Tmax = 0.961 | k = −15→15 |
| 12524 measured reflections | l = −29→29 |
Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.