Rigaku Saturn CCD area-detector diffractometer	5746 independent reflections
Radiation source: rotating anode	4491 reflections with I > 2σ(I)
multilayer	Rint = 0.048
Detector resolution: 7.31 pixels mm-1	θmax = 27.9°, θmin = 1.7°
φ and ω scans	h = −10→10
Absorption correction: multi-scan (CrystalClear; Rigaku/MSC, 2005)	k = −26→26
Tmin = 0.970, Tmax = 0.983	l = −17→20
23596 measured reflections