Bruker APEXII DUO CCD diffractometer | 28473 independent reflections |
Radiation source: fine-focus sealed tube | 20091 reflections with I > 2σ(I) |
graphite | Rint = 0.056 |
φ and ω scans | θmax = 32.4°, θmin = 1.9° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −34→34 |
Tmin = 0.758, Tmax = 0.932 | k = −26→29 |
107136 measured reflections | l = −25→27 |