| Stoe IPDS diffractometer | 1444 reflections with I > 2σ(I) |
| graphite | Rint = 0.064 |
| φ scans | θmax = 27.0°, θmin = 2.2° |
| Absorption correction: numerical (FACEIT in IPDS; Stoe & Cie, 1999) | h = −11→12 |
| Tmin = 0.188, Tmax = 0.658 | k = −9→9 |
| 6492 measured reflections | l = −14→14 |
| 1667 independent reflections |
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